Cr2Sn3S7 synthese 825°C
NPATT 1 1 <- Flags for patterns (1:refined,
0: excluded)
W_PAT 1.000
!Nph |
Dum |
Ias |
Nre |
Cry |
Opt |
Aut |
1 |
1 |
1 |
0 |
0 |
0 |
1 |
!
!File names of data(patterns) files
ch5908_Colusite_600_up_001.xy
!
! Resolution file for Pattern# 1
id21.irf
!
!Lambda1 |
Lambda2 |
Ratio |
Bkpos |
Wdt |
Cthm |
muR |
AsyLim |
Rpolarz |
2nd-muR |
0.503681 |
0.503681 |
1.00000 |
40.000 |
42.0000 |
0.0000 |
0.0000 |
3.90 |
0.0000 |
0.0000 |
!-> Patt# 1 |
!
!
!
!2Theta/TOF/E(Kev) Background for
Pattern# 1
0.5320
346.2187
0.00
0.7460
539.5665
0.00
1.2040
704.1001
0.00
1.4680
478.4053
0.00
1.6580
473.9192
0.00
1.8940
429.1152
0.00
2.1300
420.1685
0.00
2.3180
415.8386
0.00
2.5980
410.7263
0.00
2.7600
414.6676
0.00
2.9420
427.9450
0.00
3.1900
451.1159
0.00
3.4600
466.0178
0.00
3.6900
488.0145
0.00
4.1060
633.5769
0.00
4.3480
634.2810
0.00
4.4220
644.2795
0.00
4.7260
622.1424
0.00
4.8940
602.5784
0.00
5.2160
606.7883
0.00
5.4100
597.6050
0.00
5.7000
591.7344
0.00
6.0960
709.8677
0.00
6.1280
725.1663
0.00
6.3640
569.3751
0.00
!
19 !Number of refined parameters
!
!-------------------------------------------------------------------------------
! Data for PHASE number: 1
==> Current R_Bragg for Pattern#
1: 0.0000
!-------------------------------------------------------------------------------
Cu26V2Sn6S32
COMMANDS
END COMMANDS
!
!Nat |
Dis |
Ang |
Jbt |
Isy |
Str |
Furth |
ATZ |
Nvk |
More |
7 |
0 |
0 |
0 |
0 |
0 |
0 |
03491.5 |
0 |
1 |
!Jvi |
Jdi |
Hel
|
Sol |
Mom |
Ter |
0 |
0 |
0 |
0 |
0 |
0 |
!Contributions (0/1) of this phase to the 1 patterns
1
Jbt Isy Str
Furth
ATZ Nvk More
7 0
0 0 0
0
0
3491.9873 0 0
!Contributions (0/1) of this phase to the 1 patterns
!Irf |
Npr |
Jtyp |
Nsp_Ref |
Ph_Shift
|
7 |
0 |
0 |
0 |
0 |
!->Patt# 1 |
Pr1 |
Pr2 |
Pr3 |
Brind |
RMua |
RMub |
RMuc |
0.0 |
0.0 |
0.0 |
1.0 |
0.0 |
0.0 |
0.0 |
!->Patt# 1 |
!
!
P -4 3 n <--Space group symbol
!Atom Typ X Y Z Biso Occ In Fin N_t Spc /Codes
V2a
V 0.00000
0.00000 0.00000
0.47468 0.08333
0 0
0
0
0.00
0.00
0.00
111.00
0.00
Sn6c
SN 0.25000
0.50000 0.00000
1.19549
0.25000 0
0
0
0
0.00
0.00
0.00
81.00 0.00
Cu6d
CU
0.25000 0.00000
0.50000 1.56126
0.25000 0 0
0
0
0.00
0.00
0.00
141.00 0.00
Cu8e
CU
0.24755
0.24755
0.24755 1.56126
0.33333 0
0 0
0
151.00 151.00
151.00
141.00
0.00
Cu12f CU
0.25310 0.00000
0.00000 1.56126
0.50000 0
0
0
0
171.00
0.00
0.00
141.00 0.00
S8e
S
0.12395
0.12395
0.12395
0.97373 0.33333 0
0
0
0
181.00
181.00
181.00
101.00 0.00
S24i
S 0.37875
0.36764
0.12711
0.97373 1.00000 0
0
0
161.00
121.00
91.00
101.00 0.00
!-------> Profile Parameters for Pattern # 1 ----> Phase
# 1
! Scale |
Shape1 |
Bov |
Str1 |
Str2 |
Str3 |
Strain-Model |
0.14194E-06 |
1.15248 |
0.00000 |
0.00000 |
0.00000 |
0.00000 |
0 |
11.00000 |
0.000 |
0.000 |
0.000 |
0.000 |
0.000 |
0.000 |
!U |
V |
W |
X |
Y |
GauSiz |
LorSiz |
Size-Model |
0.110017 |
0.000000 |
0.000000 |
0.007515 |
0.000000 |
0.000008 |
0.000000 |
0 |
0.0 |
0.000000 |
0.000000 |
0.0 |
0.0 |
0.0 |
0.00 |
|
! a |
b |
c |
alpha |
beta |
gamma |
#Cell Info |
0.110017 |
0.000000 |
0.000000 |
0.007515 |
0.000000 |
0.000008 |
0.000000 |
0.0 |
0.0 |
0.00 |
0.0 |
0.0 |
0.0 |
0.00 |
|
! 2Th1/TOF1 2Th2/TOF2
Pattern # 1
0.902
20.000 1